N. Mufti, D.R.P. Sari, A.F. Muyasaroh, Yudyanto, Sunaryono, A. Taufiq
Nano-sized Fe3O4 has been considered prominent in material science research due to its potential applications in multi-layered aspects. One of the simple and inexpensive methods of nanosized Fe3O4 synthesis is co-precipitation. However, this method has not provided a uniform size. Therefore, this study carried out a few modifications by using PEG-200 and PEG-1000 as a soft template with a volume ratio of 1:1, 1:3, and 1:5. The Fe precursors used in this study are iron sand from the Brantas River, Kediri-East Java, Indonesia. The XRD results showed that the use of PEG in the synthesis of Fe3O4 did not affect the Fe3O4 phase, and this study obtained a crystal size with a range of 6-12 nm. Based on morphological observations using SEM, the use of soft templates in Fe3O4 synthesis can reduce agglomeration rather than without using a PEG template. All Fe3O4 powder samples showed ferrimagnetic behavior with a saturation magnetization of 39.5-70 emu/g. © Published under licence by IOP Publishing Ltd.
Department of Physics, Faculty of Mathematics and Natural Sciences, Universitas Negeri Malang, Jl. Semarang 5, Malang, 65145, Indonesia; Center of Advanced Materials for Renewable Energy (CAMRY), Universitas Negeri Malang, Jl. Semarang 5, Malang, 65145, Indonesia
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